[1]程存归,刘幸海,朱培曦.应用密闭微波辅助提取技术提取玄参中玄参苷[J].南京理工大学学报(自然科学版),2006,(02):243-247.
　CHENG Cun-gu i,L IU X ing-hai,ZHU Pe-i x i.Microwave-assisted and Airtight Solvent Extraction of Harpagoside from Radix Scrophulariae[J].Journal of Nanjing University of Science and Technology,2006,(02):243-247.
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应用密闭微波辅助提取技术提取玄参中玄参苷
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《南京理工大学学报》（自然科学版）[ISSN:1005-9830/CN:32-1397/N]

卷:
期数:
2006年02期
页码:
243-247
栏目:
出版日期:
2006-04-30

文章信息/Info

Title:
Microwave-assisted and Airtight Solvent Extraction of Harpagoside from Radix Scrophulariae
作者:
程存归1;  刘幸海2;  朱培曦1
1. 浙江师范大学化学与生命科学学院, 浙江金华321004; 2. 南开大学元素有机化学国家重点实验室, 天津300071
Author(s):
CHENG Cun-gu i1;  L IU X ing-hai2;  ZHU Pe-i x i1
1.College of Chemistry and Life Science,Zhejiang Normal University,Jinhua 321004,China;2.The State Key Laboratory of Elemento-organic Chemistry,Nankai University,Tianjin 300071,China
关键词:
玄参;  玄参苷;  密闭微波辅助提取法
Keywords:
harpagoside;  rad ix scrophu lariae;  m icrow ave-assisted and airtight so lvent extract ion
分类号:
R 284. 3
摘要:
应用密闭微波辅助提取法提取玄参中有效成分玄参苷,考察了微波提取条件(包括溶剂、样品粒径、提取时间、固-液质量体积比和提取次数等)对玄参中提取玄参苷收率的影响,结果表明:溶剂为70%乙醇,玄参的粒径为180目,提取时间为10 m in,料液比为1∶20及提取次数为2次时,玄参苷的提取率最佳。并且与常压微波辅助提取法、超声波提取法及索氏提取法进行了比较,本法具有快速、高效、绿色环保的优点。
Abstract:
The harpagoside from the rad ix scrophulariaew ere ex tracted by means ofm icrow ave-assisted and airtight so lvent ex traction. The influence of some operat ion cond itions, such as so lven,t samp le particle size, m icrow ave irradiat ion tim e, the ratio of samp le w eight to so lvent vo lume and t imes of ex tract ion, on the extraction y ield of harpagoside is studied. The experimental resu lts show that the h ighest ex traction y ield is obta ined when the extraction solvent is 70% ethano,l the sample particle size is 180 mesh, the m icrow ave irrad iation tim e is 10m in , the ratio o f samp le w eight to solvent vo lum e is 1B20 and the times o f the extraction is 2. Compared w ith the m icrow ave-assisted ex traction in norma l pressure, the ultrason ic extract ion and the soxh le t ex traction, them icrow ave-assisted extraction in c losed conta iner is fas,t effic ient and green.

参考文献/References:

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备注/Memo

备注/Memo:
基金项目: 浙江省自然科学基金( 301468) 作者简介: 程存归( 1960 - ), 浙江永康人, 副教授, 硕士生导师, 主要研究方向: 天然产物化学, E-mail:ccg@zjnu. cn。
更新日期/Last Update: 2006-04-30